SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC ： DSC6200 ・ Sample ：５ mg ・ Scan Rate ： 20 ﾟ C/min DSC.

Apresentação em tema: "SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC ： DSC6200 ・ Sample ：５ mg ・ Scan Rate ： 20 ﾟ C/min DSC."— Transcrição da apresentação:

1 SEIKO GROUP

2 ・ Sample: Azoxyanisole ・ DSC ： DSC6200 ・ Sample ：５ mg ・ Scan Rate ： 20 ﾟ C/min DSC

3 Prensinhas e Cadinhos Sample Pan 1-7 Sealed Type 8-15 Open Type 16-17 Hermetic Type Panelinhas para alta pressão DSC

4 ModeloDSC 7020DSC 6100DSC 6220DSC 6300 Tipo de DSCHeat Flux DSC Faixa de Temperatura-170 ~ 725°C-170 ~ 500°C-170 ~ 725°CAmbiente ~ 1500°C Ruído Médio0.1µW 0.2µW10µW Sensibilidade0.2µW 0.4µW20µW Taxa de Aquecimento0.01 ~ 100°C/min0.01 ~ 20°C/min0.01 ~ 100°C/min Amostrador AutomáticoOpcional Indisponível Controlador de Gás de PurgaOpcional Capacidade Máxima: Open Pan100µL 50µL Capacidade Máxima: Hermetic Sealed15µL70µL15µL Capacidade Máxima: Sealed15µL Sistema Automático de Resfriamento com LN2 (Opcional) -150 ~ 500°C -170 ~ 725°CIndisponível Sistema Eletrônico de Resfriamento (Opcional) -70 ~ 420°CC Type: -75 ~ 210°C D Type: -30 ~ 250°C C Type: -75 ~ 470°C D Type: -30 ~ 380°C Indisponível Cooling Can (Opcional)-170 ~ 725°C-170 ~ 500°C-170 ~ 725°CIndisponível DSC

5 DSC

6 DSC OVAL SENSOR Main Heat Sink Oval Sensor Plate Sample Pan Reference Pan Oval DSC Diagram Heater Oval Sensor Plate Main Heat Sink Heat Filter Lead Wire Sub Heat Sink Oval DSC Cross Section ・ High Resolution (Quick responsibility) ・ High Resolution (Quick responsibility) ・ Low thermal resistance by 2nd dimension thermo flow ・ The shortest heat flow between sample and reference ・ Protect the sensitivity down (by reducing noise lever) ・ Heat sink substrate used as sensor holder also ・ Filter stored inside sensor in order to cut the noise. DSC

7 Os DSCs da SII NanoTechnology – Seiko são os únicos DSCs com forno Elipsoidal. Melhor resolução, alta sensibilidade e excelente planicidade da linha base. Exclusividade da SEIKO SII NanoTechnology DSC

8 Full range Cooling system Electronic Cooling System, Automatic LN2 cooling system Robust Auto-sampler DSC

9 Research & Development Application ー DTG(TG) and DSC peak separation. ( for reaction of different activation energies ) ー Data simulation of measurements that are difficult such as extremely high ( ex. 10 6 ℃ /min ) or extremely low heating rates ( ex. 10 -3 ℃ /min ). Reduced measurement time for Quality Control ー Measurement time → １／２～１／１０ Application of Highway TA TG/DTA

10 Measured Data Separated Peak Synthetic Peak Peak Separation DSC

11 High and Low Heating Rate Simulation DSC